• NANOELECTROCHEMISTRY LABORATORY

Research at NECL is highly interdisciplinary, bridging across fields such as electrochemistry, analytical chemistry, materials science, nanotechnology, and surface chemistry. Our endeavors are currently centered on developing various aspects of nanomaterials through methods like wet chemistry synthesis and electrochemical techniques. Our research focuses on several interconnected domains.

• Exfoliated CoNiAl-LDH@rGO 2D/2D Heterojunction for Sustainable Hydrogen Production via Ammonia Electrolysis, Sowndharya Palanisamy, Jangwoo Shin, Sivaselvi Chellamuthu, Rajathsing Kalusulingam*, Churchil A. Antonyraj*, and Jun Ho Shim*, Energy Fuels, 2025, ASAP

• Hierarchical NiCoFe-LDH@GO nanosheet heterointerfaces for enhanced sustainable hydrogen generation via methanol- and urea-assisted water electrolysis, Eunkyung Lee,† Rajathsing Kalusulingam,† and Jun Ho Shim*, J. Electroanal. Chem., 2025, 996, 119341

• Biomass-Derived CoFe@N-doped graphitic carbon core–shell electrocatalysts for low-energy hydrogen production via methanol-ssisted water electrolysis, Rajathsing Kalusulingam, Dileep B. Pawarac, Krishnan Ravi, Selvam Mathi, Ankush V. Biradar, Tatiana N. Myasoedova, and Jun Ho Shim*, Adv. Sustainable Syst., 2025, Early View

• Hierarchical hollow microspheres assembled from sulfide-incorporated NiFe-layered double hydroxides for efficient electrocatalytic water splitting with low overpotentials, Sojin Jung, and Jun Ho Shim*, ACS Appl. Energy Mater. 2025, 8, 5259-5268

• Alkali-free single-step synthesis of delaminated layered double hydroxide in water via amino acid-assisted hydrothermal method, Paulmanickam Koilraj, Rajathsing Kalusulingam, Kannan Srinivasan,* Keiko Sasaki,* and Jun Ho Shim*, Mater. Adv. 2025, 6, 2503-2506

• Engineering MoFe nanostructures on carbon cloth for sustainable ammonia production via nitrogen reduction, Shinyoung Kweon, Nilam Qureshi,* and Jun Ho Shim*, ChemCatChem 2025, 17, e202401936